Peculiar bond characters of fivefold coordinated octet compound crystals
Chem. Sci., 2020, 11,4340-4350
DOI: 10.1039/D0SC00292E, Edge Article
DOI: 10.1039/D0SC00292E, Edge Article
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An-An Sun, Shang-Peng Gao, Gong Gu
A refreshed view of chemical bonds in solids unveils unusual bonding in fivefold coordinated bulk crystals of octet compounds: out-of-plane cation–anion chain bonding via overlapping pz orbitals replaces in-plane π bonding of the isolated monolayer.
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A refreshed view of chemical bonds in solids unveils unusual bonding in fivefold coordinated bulk crystals of octet compounds: out-of-plane cation–anion chain bonding via overlapping pz orbitals replaces in-plane π bonding of the isolated monolayer.
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SAXS studies of the thermally-induced fusion of diblock copolymer spheres: formation of hybrid nanoparticles of intermediate size and shape
Chem. Sci., 2020, 11,4312-4321
DOI: 10.1039/D0SC00569J, Edge Article
DOI: 10.1039/D0SC00569J, Edge Article
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E. J. Cornel, P. S. O'Hora, T. Smith, D. J. Growney, O. O. Mykhaylyk, S. P. Armes
Dilute dispersions of poly(lauryl methacrylate)-poly(benzyl methacrylate) diblock copolymer spheres of differing mean diameter are mixed and thermally annealed at 150 °C to produce either spherical or non-spherical nanoparticles of intermediate size.
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Dilute dispersions of poly(lauryl methacrylate)-poly(benzyl methacrylate) diblock copolymer spheres of differing mean diameter are mixed and thermally annealed at 150 °C to produce either spherical or non-spherical nanoparticles of intermediate size.
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General and selective synthesis of primary amines using Ni-based homogeneous catalysts
Chem. Sci., 2020, 11,4332-4339
DOI: 10.1039/D0SC01084G, Edge Article
DOI: 10.1039/D0SC01084G, Edge Article
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Kathiravan Murugesan, Zhihong Wei, Vishwas G. Chandrashekhar, Haijun Jiao, Matthias Beller, Rajenahally V. Jagadeesh
A Ni-triphos based homogeneous catalyst enabled the synthesis of all kinds of primary amines by reductive amination of carbonyl compounds with ammonia and hydrogenation of nitroarenes.
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A Ni-triphos based homogeneous catalyst enabled the synthesis of all kinds of primary amines by reductive amination of carbonyl compounds with ammonia and hydrogenation of nitroarenes.
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Exploiting single-electron transfer in Lewis pairs for catalytic bond-forming reactions
Chem. Sci., 2020, 11,4305-4311
DOI: 10.1039/D0SC01159B, Edge Article
DOI: 10.1039/D0SC01159B, Edge Article
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Yoshitaka Aramaki, Naoki Imaizumi, Mao Hotta, Jun Kumagai, Takashi Ooi
Radical–ion pair generation from common Lewis pairs and its application to catalytic carbon–carbon bond formation.
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Radical–ion pair generation from common Lewis pairs and its application to catalytic carbon–carbon bond formation.
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Redox-responsive supramolecular polymeric networks having double-threaded inclusion complexes
Chem. Sci., 2020, 11,4322-4331
DOI: 10.1039/C9SC05589D, Edge Article
DOI: 10.1039/C9SC05589D, Edge Article
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Hikaru Aramoto, Motofumi Osaki, Subaru Konishi, Chiharu Ueda, Yuichiro Kobayashi, Yoshinori Takashima, Akira Harada, Hiroyasu Yamaguchi
A hydrogel actuator with a 1:2 host–guest complex controlled by redox stimuli has been developed to realize faster and larger deformation.
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A hydrogel actuator with a 1:2 host–guest complex controlled by redox stimuli has been developed to realize faster and larger deformation.
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DP4-AI automated NMR data analysis: straight from spectrometer to structure
Chem. Sci., 2020, 11,4351-4359
DOI: 10.1039/D0SC00442A, Edge Article
DOI: 10.1039/D0SC00442A, Edge Article
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Alexander Howarth, Kristaps Ermanis, Jonathan M. Goodman
A robust system for automatic processing and assignment of raw 13C and 1H NMR data DP4-AI has been developed and integrated into our computational organic molecule structure elucidation workflow.
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A robust system for automatic processing and assignment of raw 13C and 1H NMR data DP4-AI has been developed and integrated into our computational organic molecule structure elucidation workflow.
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Recent developments in nickel-catalyzed intermolecular dicarbofunctionalization of alkenes
Chem. Sci., 2020, 11,4287-4296
DOI: 10.1039/C9SC06006E, Minireview
DOI: 10.1039/C9SC06006E, Minireview
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Joseph Derosa, Omar Apolinar, Taeho Kang, Van T. Tran, Keary M. Engle
Nickel-catalyzed three-component alkene difunctionalization has rapidly emerged as a powerful tool for forging multiple C–C bonds in a single step.
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Nickel-catalyzed three-component alkene difunctionalization has rapidly emerged as a powerful tool for forging multiple C–C bonds in a single step.
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Evolution of pure hydrocarbon hosts: simpler structure, higher performance and universal application in RGB phosphorescent organic light-emitting diodes
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01238F, Edge Article
DOI: 10.1039/D0SC01238F, Edge Article
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Qiang Wang, Fabien Lucas, Cassandre Quinton, Yang-Kun Qu, Joëlle Rault-Berthelot, Olivier Jeannin, Sheng-Yi Yang, Fan-Cheng Kong, Sarvendra Kumar, Liang-Sheng Liao, Cyril Poriel, Zuo-Quan Jiang
In this work, we propose pure hydrocarbon materials as universal hosts for high-efficiency red, green and blue phosphorescent organic light-emitting diodes.
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In this work, we propose pure hydrocarbon materials as universal hosts for high-efficiency red, green and blue phosphorescent organic light-emitting diodes.
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Structural trends in the dehydrogenation selectivity of palladium alloys
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00875C, Edge Article
DOI: 10.1039/D0SC00875C, Edge Article
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Stephen C. Purdy, Ranga Rohit Seemakurthi, Garrett M. Mitchell, Mark Davidson, Brooke A. Lauderback, Siddharth Deshpande, Zhenwei Wu, Evan C. Wegener, Jeffrey Greeley, Jeffrey T. Miller
Alloying is well-known to improve the dehydrogenation selectivity of pure metals, but there remains considerable debate about the structural and electronic features of alloy surfaces that give rise to this behavior.
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Alloying is well-known to improve the dehydrogenation selectivity of pure metals, but there remains considerable debate about the structural and electronic features of alloy surfaces that give rise to this behavior.
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Biofunctional Janus Particles Promote Phagocytosis of Tumor Cells by Macrophages
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01146K, Edge Article
DOI: 10.1039/D0SC01146K, Edge Article
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Ya-Ru Zhang, Jia-Qi Luo, Jia-Xian Li, Qiu-Yue Huang, Xiao-Xiao Shi, Yong-Cong Huang, Kam W Leong, Weiling He, Jinzhi Du
Herein, a versatile strategy for the construction of biofunctional Janus particles (JPs) through the combination of Pickering emulsion and copper-free click chemistry is developed for the study of particle-mediated cell-cell interactions. A...
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Herein, a versatile strategy for the construction of biofunctional Janus particles (JPs) through the combination of Pickering emulsion and copper-free click chemistry is developed for the study of particle-mediated cell-cell interactions. A...
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Rapidly Self-deoxygenating Controlled Radical Polymerization in water via in-situ Disproportionation of Cu(I)
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01512A, Edge Article
DOI: 10.1039/D0SC01512A, Edge Article
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David Haddleton, Evelina Liarou, Yisong Han, Marc Walker, Ana Sanchez
The first rapidly self-deoxygenating Cu-RDRP in aqueous media is investigated. The disproportionation of Cu(I)/Me6Tren in water towards Cu(II) and highly reactive Cu(0) leads to O2-free reaction environments within the first...
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The first rapidly self-deoxygenating Cu-RDRP in aqueous media is investigated. The disproportionation of Cu(I)/Me6Tren in water towards Cu(II) and highly reactive Cu(0) leads to O2-free reaction environments within the first...
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Regioselective B(3,4)–H Arylation of o-Carboranes by Weak Amide Coordination at Room Temperature
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01515F, Edge Article
DOI: 10.1039/D0SC01515F, Edge Article
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Yu-Feng Liang, Long Yang, Becky Bongsuiru Jei, Rositha Kuniyil, Lutz Ackermann
Palladium-catalyzed regioselective di- or mono-arylation of o-carboranes was achieved by weakly coordinating amides at room temperature. Thereby, a series of B(3,4)-diarylated and B(3)-monoarylated o-carboranes anchored with valuable functional groups were...
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Palladium-catalyzed regioselective di- or mono-arylation of o-carboranes was achieved by weakly coordinating amides at room temperature. Thereby, a series of B(3,4)-diarylated and B(3)-monoarylated o-carboranes anchored with valuable functional groups were...
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Speciation of Be2+ in acidic liquid ammonia and formation of tetra- and octanuclear beryllium amido clusters
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01112F, Edge Article
DOI: 10.1039/D0SC01112F, Edge Article
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Matthias Müller, Antti J Karttunen, Magnus Richard Buchner
The hexa-μ2-amido-tetraammine-tetraberyllium compounds [Be4(NH2)6(NH3)4]X2 (X = Cl, Br, I, CN, SCN, N3) have been prepared from beryllium metal and NH4X or [Be(NH3)4]X2 in liquid ammonia at ambient temperature. The obtained...
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The hexa-μ2-amido-tetraammine-tetraberyllium compounds [Be4(NH2)6(NH3)4]X2 (X = Cl, Br, I, CN, SCN, N3) have been prepared from beryllium metal and NH4X or [Be(NH3)4]X2 in liquid ammonia at ambient temperature. The obtained...
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Asymmetric synthesis of primary amines catalyzed by thermotolerant fungal reductive aminases
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC02253E, Edge Article
DOI: 10.1039/D0SC02253E, Edge Article
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Juan Mangas-Sanchez, Mahima Sharma, Sebastian C. Cosgrove, Jeremy I. Ramsden, James R. Marshall, Thomas W. Thorpe, Ryan B. Palmer, Gideon Grogan, Nicholas J. Turner
Fungal reductive aminases as effective biocatalysts for the preparation of chiral primary amines.
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Fungal reductive aminases as effective biocatalysts for the preparation of chiral primary amines.
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Pore engineering of ultrathin covalent organic framework membranes for organic solvent nanofiltration and molecular sieving
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01679A, Edge Article
DOI: 10.1039/D0SC01679A, Edge Article
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Digambar B. Shinde, Li Cao, A. D. Dinga Wonanke, Xiang Li, Sushil Kumar, Xiaowei Liu, Mohamed N. Hedhili, Abdul-Hamid Emwas, Matthew Addicoat, Kuo-Wei Huang, Zhiping Lai
Pore surface engineering of ultrathin COF membranes by introducing different lengths of alkyl chains into the skeleton, which allows us to precisely control the pore size of COF membranes for OSN applications and molecular sieving.
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Pore surface engineering of ultrathin COF membranes by introducing different lengths of alkyl chains into the skeleton, which allows us to precisely control the pore size of COF membranes for OSN applications and molecular sieving.
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Highly efficient non-doped blue fluorescent OLEDs with low efficiency roll-off based on hybridized local and charge transfer excited state emitters
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01341B, Edge Article
DOI: 10.1039/D0SC01341B, Edge Article
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Xianhao Lv, Mizhen Sun, Lei Xu, Runzhe Wang, Huayi Zhou, Yuyu Pan, Shitong Zhang, Qikun Sun, Shanfeng Xue, Wenjun Yang
A new pure fluorescent blue HLCT-emitter was designed and synthesized. Highly efficient non-doped blue OLEDs with low efficiency roll-off were achieved.
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A new pure fluorescent blue HLCT-emitter was designed and synthesized. Highly efficient non-doped blue OLEDs with low efficiency roll-off were achieved.
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Nickel catalysis enables convergent paired electrolysis for direct arylation of benzylic C–H bonds
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01445A, Edge Article
DOI: 10.1039/D0SC01445A, Edge Article
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Lei Zhang, Xile Hu
A direct arylation of benzylic C–H bonds is achieved by integrating Ni-catalyzed benzyl–aryl coupling into convergent paired electrolysis.
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A direct arylation of benzylic C–H bonds is achieved by integrating Ni-catalyzed benzyl–aryl coupling into convergent paired electrolysis.
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Structure and redox tuning of gas adsorption properties in calixarene-supported Fe(II)-based porous cages
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01833C, Edge Article
DOI: 10.1039/D0SC01833C, Edge Article
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Meaghan Deegan, Tonia Ahmed, Glenn Yap, Eric D Bloch
We describe the synthesis of Fe(II)-based octahedral coordination cages supported by calixarene capping ligands. The most porous of these molecular cages has an argon accessible BET surface area of 898...
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We describe the synthesis of Fe(II)-based octahedral coordination cages supported by calixarene capping ligands. The most porous of these molecular cages has an argon accessible BET surface area of 898...
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Protease-Responsive Mass Barcoded Nanotranslaters for Simultaneously Quantifying the Intracellular Activity of Cascaded Caspases in Apoptosis Pathways
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01534B, Edge Article
DOI: 10.1039/D0SC01534B, Edge Article
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Hongmei Xu, Xiaodan Huang, Zhenzhen Zhang, xuemeng zhang, Qianhao Min, Jun-Jie Zhu
Quantitatively delineating the activation network of multiple proteases that participate in cellular processes is highly essential to understanding physiological and pathological states of cells. In this study, protease-responsive mass barcoded...
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Quantitatively delineating the activation network of multiple proteases that participate in cellular processes is highly essential to understanding physiological and pathological states of cells. In this study, protease-responsive mass barcoded...
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Ring-Fused Cyclobutanes via Cycloisomerization of Alkylidenecyclopropane Acylsilanes
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC02224A, Edge Article
DOI: 10.1039/D0SC02224A, Edge Article
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Erick M Carreira, Sarah S Eichenberger, Moritz Hönig, Matthieu JR Richter, Renana Gershoni-Poranne
A novel Lewis acid-catalyzed cycloisomerization of alkylidenecyclopropane acylsilanes is disclosed. The readily available starting materials participate in tandem Prins addition/ring expansion/1,2-silyl shift to grant access to bicyclo[4.2.0]octanes and bicyclo[3.2.0]heptanes, which...
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A novel Lewis acid-catalyzed cycloisomerization of alkylidenecyclopropane acylsilanes is disclosed. The readily available starting materials participate in tandem Prins addition/ring expansion/1,2-silyl shift to grant access to bicyclo[4.2.0]octanes and bicyclo[3.2.0]heptanes, which...
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Stereo-controlled anti-hydromagnesiation of aryl alkynes by magnesium hydrides
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01773F, Edge Article
DOI: 10.1039/D0SC01773F, Edge Article
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Bin Wang, Derek Yiren Ong, Yihang Li, Jia Hao Pang, Kohei Watanabe, Ryo TAKITA, Shunsuke Chiba
A concise protocol for anti-hydromagnesiation of aryl alkynes was established using 1:1 molar combination of sodium hydride (NaH) and magnesium iodide (MgI2) without the aid of any transition metal catalysts....
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A concise protocol for anti-hydromagnesiation of aryl alkynes was established using 1:1 molar combination of sodium hydride (NaH) and magnesium iodide (MgI2) without the aid of any transition metal catalysts....
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Triblock polyester thermoplastic elastomers with semi-aromatic polymer end blocks by ring-opening copolymerization
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00463D, Edge Article
DOI: 10.1039/D0SC00463D, Edge Article
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Georgina L. Gregory, Gregory S. Sulley, Leticia Peña Carrodeguas, Thomas T. D. Chen, Alba Santmarti, Nicholas J. Terrill, Koon-Yang Lee, Charlotte K. Williams
A new series of block polyester thermoplastic elastomers are prepared by a one-pot procedure; they show properties competitive or better than conventional materials and can be fully degraded after use.
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A new series of block polyester thermoplastic elastomers are prepared by a one-pot procedure; they show properties competitive or better than conventional materials and can be fully degraded after use.
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Expedient synthesis of conjugated triynes via alkyne metathesis
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01124J, Edge Article
DOI: 10.1039/D0SC01124J, Edge Article
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Idriss Curbet, Sophie Colombel-Rouen, Romane Manguin, Anthony Clermont, Alexandre Quelhas, Daniel S. Müller, Thierry Roisnel, Olivier Baslé, Yann Trolez, Marc Mauduit
The first synthesis of symmetrical and dissymmetrical conjugated triynes by self- and cross-metathesis was successfully achieved thanks to the use of hindered diynes.
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The first synthesis of symmetrical and dissymmetrical conjugated triynes by self- and cross-metathesis was successfully achieved thanks to the use of hindered diynes.
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Efficient alkene hydrosilation with bis(8-quinolyl)phosphine (NPN) nickel catalysts. The dominant role of silyl-over hydrido-nickel catalytic intermediates
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00997K, Edge Article
DOI: 10.1039/D0SC00997K, Edge Article
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Jian Yang, Verònica Postils, Michael I. Lipschutz, Meg Fasulo, Christophe Raynaud, Eric Clot, Odile Eisenstein, T. Don Tilley
A cationic nickel complex of the bis(8-quinolyl)(3,5-di-tert-butylphenoxy)phosphine (NPN) ligand, [(NPN)NiCl]+, is a precursor to efficient catalysts for the hydrosilation of alkenes with hydrosilanes under mild conditions and low catalyst loadings.
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A cationic nickel complex of the bis(8-quinolyl)(3,5-di-tert-butylphenoxy)phosphine (NPN) ligand, [(NPN)NiCl]+, is a precursor to efficient catalysts for the hydrosilation of alkenes with hydrosilanes under mild conditions and low catalyst loadings.
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Molecular recognition of pyrazine N,N'-dioxide using aryl extended calix[4]pyrroles
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01496F, Edge Article
DOI: 10.1039/D0SC01496F, Edge Article
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Chenxing Guo, Hu Wang, Vincent M. Lynch, Xiaofan Ji, Zachariah A. Page, Jonathan L. Sessler
The molecular recognition of pyrazine N,N'-dioxide by aryl extended 'two-walled' calix[4]pyrrole-based receptors is seen to stabilise two different binding modes in the solid state.
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The molecular recognition of pyrazine N,N'-dioxide by aryl extended 'two-walled' calix[4]pyrrole-based receptors is seen to stabilise two different binding modes in the solid state.
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Metal-metal cooperative bond activation by heterobimetallic alkyl, aryl, and acetylide PtII/CuI complexes
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC00646G, Edge Article
DOI: 10.1039/D0SC00646G, Edge Article
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Shubham Deolka, Orestes Rivada, Sandra L. Aristizábal, Robert R. Fayzullin, Shrinwantu Pal, Kyoko Nozaki, Eugene Khaskin, Julia R Khusnutdinova
We report selective formation of heterobimetallic PtII/CuI complexes that demonstrate how facile bond activation processes can be achieved by altering reactivity of common organoplatinum compounds through their interaction with another...
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We report selective formation of heterobimetallic PtII/CuI complexes that demonstrate how facile bond activation processes can be achieved by altering reactivity of common organoplatinum compounds through their interaction with another...
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Structure of Copper sites in Zeolites Examined by Fourier and Wavelet Transform Analysis of EXAFS
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01472A, Edge Article
DOI: 10.1039/D0SC01472A, Edge Article
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Vitaly L. Sushkevich, Olga V. Safonova, Dennis Palagin, Mark A Newton, Jeroen van Bokhoven
Copper-exchanged zeolites are a class of redox-active materials that find application in the selective catalytic reduction of exhaust gases of diesel vehicles, and, more recently, the selective oxidation of methane...
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Copper-exchanged zeolites are a class of redox-active materials that find application in the selective catalytic reduction of exhaust gases of diesel vehicles, and, more recently, the selective oxidation of methane...
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Dynamic reaction-induced phase separation in tunable, adaptive covalent networks
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00605J, Edge Article
DOI: 10.1039/D0SC00605J, Edge Article
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Katie M. Herbert, Patrick T. Getty, Neil D. Dolinski, Jerald E. Hertzog, Derek de Jong, James H. Lettow, Joy Romulus, Jonathan W. Onorato, Elizabeth M. Foster, Stuart J. Rowan
Dynamic covalent networks comprised of tunable thia-Michael bonds result in phase separated networks with tailorable mechanical and adaptive properties.
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Dynamic covalent networks comprised of tunable thia-Michael bonds result in phase separated networks with tailorable mechanical and adaptive properties.
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A straightforward approach to antibodies recognising cancer specific glycopeptidic neoepitopes
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00317D, Edge Article
DOI: 10.1039/D0SC00317D, Edge Article
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Hajime Wakui, Yoshikazu Tanaka, Toyoyuki Ose, Isamu Matsumoto, Koji Kato, Yao Min, Taro Tachibana, Masaharu Sato, Kentaro Naruchi, Fayna Garcia Martin, Hiroshi Hinou, Shin-Ichiro Nishimura
We developed new class of designated antibodies targeting of “dynamic neoepitopes” elaborated by disease-specific O-glycosylation at the immunodominant mucin domains.
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We developed new class of designated antibodies targeting of “dynamic neoepitopes” elaborated by disease-specific O-glycosylation at the immunodominant mucin domains.
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Water-induced formation of an alkali-ion dimer in cryptomelane nanorods
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01517B, Edge Article
DOI: 10.1039/D0SC01517B, Edge Article
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Shaobo Cheng, Vidushi Sharma, Altug S. Poyraz, Lijun Wu, Xing Li, Amy C. Marschilok, Esther S. Takeuchi, Kenneth J. Takeuchi, Marivi Fernández-Serra, Yimei Zhu
Water displaces potassium ions and initiates the formation of a homonuclear dimer ion (K2+) in the tunnels of hollandite.
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Water displaces potassium ions and initiates the formation of a homonuclear dimer ion (K2+) in the tunnels of hollandite.
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Introduction of a 7-aza-6-MeO-indoline auxiliary in Lewis-acid/photoredox cooperative catalysis: highly enantioselective aminomethylation of α,β-unsaturated amides
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01890B, Edge Article
DOI: 10.1039/D0SC01890B, Edge Article
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Santosh K. Pagire, Naoya Kumagai, Masakatsu Shibasaki
An efficient cooperative chiral Lewis acid and photoredox catalytic system towards the highly enantioselective radical conjugate addition of α-amino radicals to α,β-unsaturated amides is developed with the implementation of unique auxiliaries.
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An efficient cooperative chiral Lewis acid and photoredox catalytic system towards the highly enantioselective radical conjugate addition of α-amino radicals to α,β-unsaturated amides is developed with the implementation of unique auxiliaries.
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Nitric oxide monooxygenation (NOM) reaction of cobalt-nitrosyl {Co(NO)}8 to CoII-nitrito {CoII(NO2−)}: base induced hydrogen gas (H2) evolution
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01572E, Edge Article
DOI: 10.1039/D0SC01572E, Edge Article
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Sandip Das, Kulbir, Somnath Ghosh, Subash Chandra Sahoo, Pankaj Kumar
Base-induced hydrogen (H2) gas evolution in the nitric oxide monoxygenation reaction.
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Base-induced hydrogen (H2) gas evolution in the nitric oxide monoxygenation reaction.
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Programmable synthesis of multiply arylated cubanes through C–H metalation and arylation
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01909G, Edge Article
DOI: 10.1039/D0SC01909G, Edge Article
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Ryo Okude, Genki Mori, Akiko Yagi, Kenichiro Itami
Cubane has attracted attention due to its unique 3D structure. Herein, we report the programmable synthesis of multiply arylated cubanes. The developed reaction allows the late-stage and regioselective installation of aryl groups.
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Cubane has attracted attention due to its unique 3D structure. Herein, we report the programmable synthesis of multiply arylated cubanes. The developed reaction allows the late-stage and regioselective installation of aryl groups.
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Thermal effects – an alternative mechanism for plasmon-assisted photocatalysis
Chem. Sci., 2020, Advance Article
DOI: 10.1039/C9SC06480J, Edge Article
DOI: 10.1039/C9SC06480J, Edge Article
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Yonatan Dubi, Ieng Wai Un, Yonatan Sivan
A simple Arrhenius-based theory of heating, rather than “hot electrons”, can reproduce some high-profile photocatalysis experimental results to remarkable accuracy. Flaws in temperature measurement may have led to wrong conclusions.
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A simple Arrhenius-based theory of heating, rather than “hot electrons”, can reproduce some high-profile photocatalysis experimental results to remarkable accuracy. Flaws in temperature measurement may have led to wrong conclusions.
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Crystallographic facet selective HER catalysis: exemplified in FeP and NiP2 single crystals
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00676A, Edge Article
DOI: 10.1039/D0SC00676A, Edge Article
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Bryan Owens-Baird, Juliana P. S. Sousa, Yasmine Ziouani, Dmitri Y. Petrovykh, Nikolai A. Zarkevich, Duane D. Johnson, Yury V. Kolen'ko, Kirill Kovnir
The effect of the crystal structure of ordered transition-metal phosphide catalysts on the hydrogen-evolution reaction is investigated using single crystals of iron-phosphide (FeP) and monoclinic nickel-diphosphide (m-NiP2).
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The effect of the crystal structure of ordered transition-metal phosphide catalysts on the hydrogen-evolution reaction is investigated using single crystals of iron-phosphide (FeP) and monoclinic nickel-diphosphide (m-NiP2).
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Covalent Organic Frameworks as Microreactors: Confinement-enhanced Electrochemiluminescence
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01817A, Edge Article
DOI: 10.1039/D0SC01817A, Edge Article
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Wei-Jia Zeng, Kun Wang, Wenbin Liang, Yaqin Chai, Ruo Yuan, Ying Zhuo
Herein, the electrochemiluminescence (ECL) microreactors with enhanced intensity and extreme stability were firstly established by the assembly of tris(2,2’-bipyridyl) ruthenium (II) (Ru(bpy)32+) onto the covalent organic frameworks (COFs) where a...
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Herein, the electrochemiluminescence (ECL) microreactors with enhanced intensity and extreme stability were firstly established by the assembly of tris(2,2’-bipyridyl) ruthenium (II) (Ru(bpy)32+) onto the covalent organic frameworks (COFs) where a...
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Ultrafast Amidation of Esters using Lithium Amides under Aerobic Ambient Temperature Conditions in Sustainable Solvents
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01349H, Edge Article
DOI: 10.1039/D0SC01349H, Edge Article
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Michael Fairley, Leonie Bole, Florian Mulks, Laura Main, Alan Kennedy, Charles T. O'Hara, Joaquín García-Álvarez, Eva Hevia
Lithium amides constitute one of the most commonly used class of reagents in synthetic chemisty. However, despite many applications, their use is handicapped by their requirements of low temperatures, in...
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Lithium amides constitute one of the most commonly used class of reagents in synthetic chemisty. However, despite many applications, their use is handicapped by their requirements of low temperatures, in...
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Transformation from helical to layered supramolecular organization of asymmetric perylene diimides via multiple intermolecular hydrogen bonding
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01911A, Edge Article
DOI: 10.1039/D0SC01911A, Edge Article
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Mengmeng Li, Wojciech Zajaczkowski, Gangamallaiah Velpula, Daniel Jänsch, Robert Graf, Tomasz Marszalek, Sapun H. Parekh, Yulian Zagranyarski, Kunal Mali, Manfred Wagner, Steven De Feyter, Chen Li, Klaus Müllen, Wojciech Pisula
The solid-state supramolecular organization of asymmetric perylene diimide is transformed from helical to layered self-assembly after thermal annealing.
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The solid-state supramolecular organization of asymmetric perylene diimide is transformed from helical to layered self-assembly after thermal annealing.
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Allylic C(sp3)–H alkylation via synergistic organo- and photoredox catalyzed radical addition to imines
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00819B, Edge Article
DOI: 10.1039/D0SC00819B, Edge Article
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Jiaqi Jia, Rajesh Kancherla, Magnus Rueping, Long Huang
A new catalytic method for the direct alkylation of allylic C(sp3)–H bonds from unactivated alkenes via synergistic organo- and photoredox catalysis is described.
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A new catalytic method for the direct alkylation of allylic C(sp3)–H bonds from unactivated alkenes via synergistic organo- and photoredox catalysis is described.
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Palladium-catalysed 5-endo-trig allylic (hetero)arylation
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01932A, Edge Article
DOI: 10.1039/D0SC01932A, Edge Article
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Bara Singh, Siddheshwar K. Bankar, Ketan Kumar, S. S. V. Ramasastry
A palladium-catalysed intramolecular allylic (hetero)arylation strategy for the synthesis of fused cyclopentenes incorporated with all-carbon quaternary and spiro centres is described.
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A palladium-catalysed intramolecular allylic (hetero)arylation strategy for the synthesis of fused cyclopentenes incorporated with all-carbon quaternary and spiro centres is described.
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Spontaneous mirror symmetry breaking in benzil-based soft crystalline, cubic liquid crystalline and isotropic liquid phases
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01396J, Edge Article
DOI: 10.1039/D0SC01396J, Edge Article
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Tino Reppe, Silvio Poppe, Xiaoqian Cai, Yu Cao, Feng Liu, Carsten Tschierske
Benzil (diphenylethane-1,2-dione), which is a long known example for an achiral molecule crystallizing in a chiral space group, can also show mirror symmetry breaking in the fluid state if it...
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Benzil (diphenylethane-1,2-dione), which is a long known example for an achiral molecule crystallizing in a chiral space group, can also show mirror symmetry breaking in the fluid state if it...
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When Hollow Multi-Shelled Structures (HoMSs) Meet Metal-Organic Frameworks (MOFs)
Chem. Sci., 2020, Accepted Manuscript
DOI: 10.1039/D0SC01284J, Perspective
DOI: 10.1039/D0SC01284J, Perspective
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Zumin Wang, Nailiang Yang, Dan Wang
Hollow multishelled structures (HoMSs) have distinguished advantages, such as large effective surface area, short mass transport route, and high loading capacity, but the fabrication of HoMS was a big challenge....
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Hollow multishelled structures (HoMSs) have distinguished advantages, such as large effective surface area, short mass transport route, and high loading capacity, but the fabrication of HoMS was a big challenge....
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Aerosol-assisted route to low-E transparent conductive gallium-doped zinc oxide coatings from pre-organized and halogen-free precursor
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00502A, Edge Article
DOI: 10.1039/D0SC00502A, Edge Article
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Clara Sanchez-Perez, Sebastian C. Dixon, Jawwad A. Darr, Ivan P. Parkin, Claire J. Carmalt
A pre-organised and halogen-free ZnO precursor is used to deposit GZO coatings via aerosol-assisted CVD with properties that exceed industrial standards for low-E coatings and photovoltaics.
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A pre-organised and halogen-free ZnO precursor is used to deposit GZO coatings via aerosol-assisted CVD with properties that exceed industrial standards for low-E coatings and photovoltaics.
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The assemble, grow and lift-off (AGLO) strategy to construct complex gold nanostructures with pre-designed morphologies
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00553C, Edge Article
DOI: 10.1039/D0SC00553C, Edge Article
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Xin Luo, Christophe Lachance-Brais, Amy Bantle, Hanadi F. Sleiman
The AGLO strategy generates complex gold nanostructures with user-designed morphologies in solution, using only a simple 2D DNA origami sheet as a versatile transient template. The products are robust and stable as standalone gold nanostructures.
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The AGLO strategy generates complex gold nanostructures with user-designed morphologies in solution, using only a simple 2D DNA origami sheet as a versatile transient template. The products are robust and stable as standalone gold nanostructures.
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Structure-mechanics statistical learning unravels the linkage between local rigidity and global flexibility in nucleic acids
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00480D, Edge Article
DOI: 10.1039/D0SC00480D, Edge Article
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Yi-Tsao Chen, Haw Yang, Jhih-Wei Chu
The mechanical properties of nucleic acids underlie biological processes ranging from genome packaging to gene expression. We devise structural mechanics statistical learning method to reveal their molecular origin in terms of chemical interactions.
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The mechanical properties of nucleic acids underlie biological processes ranging from genome packaging to gene expression. We devise structural mechanics statistical learning method to reveal their molecular origin in terms of chemical interactions.
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Evolutionary chemical space exploration for functional materials: computational organic semiconductor discovery
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00554A, Edge Article
DOI: 10.1039/D0SC00554A, Edge Article
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Chi Y. Cheng, Josh E. Campbell, Graeme M. Day
Evolutionary optimisation and crystal structure prediction are used to explore chemical space for molecular organic semiconductors.
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Evolutionary optimisation and crystal structure prediction are used to explore chemical space for molecular organic semiconductors.
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Retrosynthetic strategies and their impact on synthesis of arcutane natural products
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01441A, Minireview
DOI: 10.1039/D0SC01441A, Minireview
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Shelby V. McCowen, Nicolle A. Doering, Richmond Sarpong
Decisions, decisions, decisions: the interplay between different retrosynthetic strategies in the synthesis of the highly bridged, polycyclic arcutane natural products.
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Decisions, decisions, decisions: the interplay between different retrosynthetic strategies in the synthesis of the highly bridged, polycyclic arcutane natural products.
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Spectroscopic investigations under whole-cell conditions provide new insight into the metal hydride chemistry of [FeFe]-hydrogenase
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC00512F, Edge Article
DOI: 10.1039/D0SC00512F, Edge Article
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Lívia S. Mészáros, Pierre Ceccaldi, Marco Lorenzi, Holly J. Redman, Emanuel Pfitzner, Joachim Heberle, Moritz Senger, Sven T. Stripp, Gustav Berggren
The mechanism of hydrogen gas formation by [FeFe] hydrogenase is probed under whole cell conditions, revealing the formation of reactive metal hydride species under physiologically relevant conditions.
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The mechanism of hydrogen gas formation by [FeFe] hydrogenase is probed under whole cell conditions, revealing the formation of reactive metal hydride species under physiologically relevant conditions.
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Copper-catalysed photoinduced decarboxylative alkynylation: a combined experimental and computational study
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC02213F, Edge Article
DOI: 10.1039/D0SC02213F, Edge Article
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Yu Mao, Wenxuan Zhao, Shuo Lu, Lei Yu, Yi Wang, Yong Liang, Shengyang Ni, Yi Pan
Redox-active esters (RAEs) as alkyl radical precursors have demonstrated great advantages for Cu-catalysed C–C bond formation.
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Redox-active esters (RAEs) as alkyl radical precursors have demonstrated great advantages for Cu-catalysed C–C bond formation.
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Cascade polymerizations: recent developments in the formation of polymer repeat units by cascade reactions
Chem. Sci., 2020, Advance Article
DOI: 10.1039/D0SC01475C, Perspective
DOI: 10.1039/D0SC01475C, Perspective
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Gregory I. Peterson, Tae-Lim Choi
Cascade polymerizations provide new routes to unique polymer structures. In this perspective, we summarize their performance, monomer scope, and mechanisms.
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Cascade polymerizations provide new routes to unique polymer structures. In this perspective, we summarize their performance, monomer scope, and mechanisms.
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